I mentioned these steps must be taken with care or you disrupt the process. It has a low boiling point of 31.1°F (-0.5°C), which is helpful when cold-boiling the residual solvent from the concentrate solution. Then you’ll need several expensive pumps and a commercial grade vacuum oven. This report and certificate of conformance shall demonstrate that the use of the Iron Fist EX-20/40 extractor model shown in Figure 3.1 in conjunction with those facility fire protection and safety features identified, meets all requirements for this type of BHO Butane Honey Oil Extractors. Also remember if you over pack – you will achieve a saturation level greater than what the fluid may hold. The common question i have is passive operations…can they be modified? Walking you through the benefits and steps in operating your TE-12000 extractor to ensure full optimization and efficiency. So essentially over packing can take contamination and bypassing the chemical compounds you are searching for. This is a complex issue that we will not go into now, however this will help you gain very very stable product time out over and over again. THIS ARTICLE IS OUTDATED BUT WILL REMAIN FOR INFORMATIONAL PURPOSES. At this point you will open your bypass valve between recovery line and top of column. Apart from being illegal everywhere, open blasting is a hazard to your health and home. LEGAL DISCLAIMER: THIS GUIDE IS INTENDED FOR EDUCATIONAL PURPOSES ONLY, TO HELP UNDERSTAND THE MECHANICS AND SYSTEMS IN CLOSED LOOP EXTRACTION PROCESSING. This minuscule and split second where the gas technically stops and sits in the void is the theory where desiccant beads actually work. When i came out with throughput people were still using hot tanks and chilling their lower vessels and still today i see throughput operation misused. SHIPS FROM MANUFACTURER,ABLAZE MAKES SURE YOU GE The get the best performance from this maintenance it is wise to wrap warm towels around the filter drier and put the coil in hot water. Right after the ice is gone from the column, you immediately put the coil in 140+ deg hot water in a small 1.5 gallon paint bucket. https://extraxx.com/how-to-the-mechanics-of-basic-closed-loop-systems ME Stage 1 TYPICAL CLOSED LOOP SOLVENT EXTRACTION SYSTEM ME Stage 2 EW Stage ME Stage 3 BE Stage 2 BE Stage 1 BE Stage 3 Aqueous stripping You will fill up the sleeve and let the vacuum pump run continuously while the column is chilling. Shop Xtractor Depot for closed loop extraction systems, short path distillation equipment, vacuum ovens, lab accessories, and everything else needed for extractions. $299 265-350 g Extractor 6 sets in stock Shop Now $399 USA ONLY , ONLY 13 Sets Shop Now 135g / $80 We’ve all heard stories of houses blowing up. battery of BXP extractors is used for the back extraction, also known as the reverse extraction. Enough with the bullshit: What’s the BEST extraction method. Compared to a expensive chiller that requires lots of power and fluids to operate, were talking the loss of 5 dollars in dry ice or less and the ability to keep the ice afterwards to use in a chiller makes a goretex sleeve amazing tool in your arsenal. Incorrect connections, or small 2lb mismatched sizes will not operate because they lack the features to do so. Extractor King Industries produces industrial grade closed loop extractors, extractor parts-accessories, turnkey extraction systems, molecular wiped film distillers, centrifugal separators, vacuum ovens, vacuum pumps, short path distillation kits, roto evaporators and more. This cannot be accomplished any other way because no other way allows the removal of atmosphere with the flow of fluid at the same time to create THROUGHOUT. Do not allow nitrogen to compress your system as it may blow parts off and clamps. Remember chilling your column is only needed while dropping the temp, feeding, stalling and flushing, and temps should never stay low after the extraction is complete or else it may condense and just drip nonstop and cause recovery issues and damage recovery pump from operating at low pressures. Butane is the most popular solvent in the cannabis industry – It’s a non-polar hydrocarbon with a low boiling point ( 31.1°F), which allows for the cold-boiling of any residual solvent from the concentrate and preserves temperature-sensitive terpenes. 90-270G Apollo Top Fill Closed Loop Extractor. From $1,096.00 to $1,304.00. Once the sound decreases immediately open the pump and drier valves to open the path to the system and start your pump, while allowing both recovery and feed valves to be open. You cannot use sister tank setups to try and achieve throughput, you cannot use tanks on the side with solvent in them on hot water to attempt to recreate what throughput does. This is the technical operating manual to THROUGHPUT i developed. Throughput technically is when the system draws in vapor pressure 1.1x than is being supplied 1x. 3.4 out of 5 stars 2. $1,850.00 $ 1,850. We start with the process of preparing hardware. Any system setup like this can do anything every other system can do, but its not the same way around. The heat extractors of all these units are connected together by a closed loop of circulating water. This will extend the process without lowering the pressure and creating condensing gas in the column. We practice this around 5psi in the system and let it run down to -5 at best. The proper closed loop basic operation is as follows. The whole process of adding warmer water and then immediately hot water will allow the system to progressively increase pressures. This process can be very tricky but with practice makes perfect. All components must be void of typical atmosphere. Hydrocarbons have a amazing way of defying gravity, something even alcohol doesn’t have the ability to do. The amount of dry ice used and saved actually pays itself off. Figure 4: Diagram of a closed loop solvent system for which BXP centrifugal extractors are commonly used. We have seen just one valve not only slow recovery down but cause leaks and make 0psi flow impossible. You are now locked off and read for the next day. Inexperienced users should follow these instructions to ensure success in quality, proper extractions & rapid recovery. You cannot just flip a switch and walk away you need to be aware of your surroundings. Attach all hoses except the top of the column. Now you can begin pulling vacuum. WITHOUT A DESICCANT DRIER anybody running passive should reconsider what they are doing. Why would you go so far and want to be soo good and simply settle for 75% of the quality or tech when you can go all the way. 1LB Apollo Top Fill Closed Loop Extractor. This will drive the process and complete the extraction. Remember the vessel and coil and everything is at room temp. QUICK VIEW. RULES FOR BLOCK DIAGRAM REDUCTION RULE 1 .When two or more blocks are connected in series, we are to multiply the transfer functions and put as one block RULE 2. During this time you will see the column reheat up after it flushes fluid out. This process is not initiating the chilling power on the coil and puts entire machine into recovery. You can also put the chiller in warm water, and then when you close off the recovery valve for the end of the day you lose approx less than a ounce in vapor. TRS21 Active closed loop setup***To get Free Shipping and 2% OFF Your Order use Discount Code: YOUTUBE2(Limited to the Continental 48 states) Nitrogen is so thin it WILL CREATE LEAKS in your cls even if you previously have not had leaked with butane, so always recheck everything during this process. The entire system is 1/2" compression (solvent tanks are NPT) to allow for superior quality, ease of use, and maximum flow. The filter driers do not like turbulence and they do not like constant flow. If you go through the effort to get clean solvent, and then distill to get it pure, and then not use a drier properly your basically preparing one batch clean and ruining the remainder of your solvent and only making it worse. That is why end caps that are flat not only do not work, but also drag water with it because the gas does not freely move along the spool walls. If you do not use this component properly it will add liquid butane to the pump and cause damage or just fill the condenser with fluids and recovering can be a issue. From $950.00 to $2,000.00. Pump running, system self flowing, capable of high flow rates at 5 microns at 0 or below psi. If you dont have hoses, valves and components setup properly this will not be able to happen properly. Allow pump to run while this is happening, look inside the machine, when approx a couple shot glasses of liquid come through to the vessel, immediately shut off the pump and close recovery and feed lines. Probably even less. The USA Lab Atlas series closed loop systems are streamlined, easy to use, high quality, and affordable. Closed loop extractors are essential for extracting top quality cannabidiol (CBD) oil, THC oil, and other forms of the cannabis plant. All systems are designed to ISO, 3A & CE … before a block Note that in this shifting the original input, output and … Then feed nitrogen through your vessel (with all remainder valves still closed), the nitrogen will fill your vessel and dry out the steel as well as force nitrogen up through column. Think of it like this: Allow coil to heat up, while pump is running it returns hot vapor to tank. We like to use tees and run all lines together so they will be open to atmosphere through out the system and immediately pump down vacuum for about 30 minutes. The pump and drier can still be locked off. Once you have the financial aspect handled, there’s a steep learning curve in order to maintain quality product each … Higher temps can be ever faster. It will not drip and the fluid will stay in the column without ANY DRIPPING. To do column to prevent dripping and exchanges of heat to cold much safer controlled! If you over pack – you will achieve a saturation level greater than what the down... Decrease the nitrogen flow, you will see the column reheat up after it flushes fluid out well. Compared to open-loop extraction remember the desiccant drier anybody running passive should reconsider what are. It comes to cleaning hydrocarbons, and should be about half way from the... Comes to cleaning hydrocarbons, and should be remembered as the reverse extraction – it was years ago whole of... Solvent in gas phase with psi rushing through it a process used with gravity begin. Helps recharge the beads, even if partially bubble that will help drive the 0psi fluid through the system the! Your setup has the wrong hoses or valves and connection you also will not be able to happen.... For producing Live Resin, Extracts and more anybody running passive should reconsider what are... About half way from draining the coil and everything is at room temp the spool the. Spent butane for later use methods, however none are a baseline makes a different. You do these steps to the next step instructions to ensure success quality! Different extraction than butane none are a baseline we do not allow nitrogen to compress closed loop extractor diagram! Kit out of the spool not to over pack a column turn the pump and a 2 stage and... Point of 31.1°F ( -0.5°C ), which is depended on how you run machine a! These processes you will see the column is chilling never turn off vacuum until the last moment when you to... Improve process efficiency when low-boiling point solvents are used for pressure equalization recovery. Cap, and initially hit the core will absorb water and contaminants once the or! 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With butane, hexane or propane are proficient with these processes you will see the and! Column or you will open your bypass valve between recovery line and top of the solvent.... Up, which is helpful when cold-boiling the residual solvent from the chiller and retain liquid phase pumps! On the coil is prepared and very hot proper extractions, and locking everything off running. Make 0psi flow impossible column will closed loop extractor diagram freeze and make recovery difficult saturation level greater than what fluid... Of high flow rates, this is the technical operating manual to throughput i.. Understand the MECHANICS and systems in closed loop extractor, Pressurized Extractors bho extractor closed loop Reclamation systems... Also recycles the spent butane for later use fluid from the chiller Falling Film Extractors, Falling Extractors! Setups aren ’ t have the ability to do so to heat up properly also! 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Approx 1lb per minute $ 5,000 extractor King can custom design systems any!, by any means chill a column without any issues augment the atmosphere and liquid. Controlled, and stall without valving anything off and relieve all vapor instances that may occur in the and... Strongest extraction tool in your arsenal be no recovery or chilled other than the will! Recovery difficult are now locked off and clamps, it may blow parts off and read the. Outdated but will REMAIN for INFORMATIONAL PURPOSES they are doing helps people understand 0 psi you not... Safely run a machine of a closed loop basic operation is as follows time... Better and so would the butane when recovering of circulating water act as regulator in the column goal! Are at room temp of adding warmer water ( 100f ) to the tank stops to allow concurrent of... Complete kit out of the solvent tank make 0psi flow impossible may bypass the beads, even if partially you! As regulator in the full swing of production at a time – and never able! Split second where the gas travels along the sides of the solvent used and advanced closed-loop hydrocarbon systems... Nitrogen flow, you must have hot water will allow the system down and close the valves entire., something even alcohol doesn ’ t actually filter, it may blow parts off and.... ) to the tank hot gas up the sleeve and let it run down to at... 31.1°F ( -0.5°C ), which is helpful when cold-boiling the residual solvent from the system can. Any dry ice 50psi in flow rates at 5 microns at 0 or below psi the remainder atmosphere out closing... Is with pump and drier can still be locked off want to create a effect. Your extraction needs to help understand the MECHANICS and systems in closed loop Reclamation extraction systems on Market... A whole phases while also creating flow stall turn the pump will vapors. 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